Volume 1, Issue 2, December 2017, Page: 34-39
Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds
Joumaa Merza, Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria
Ali Alasmi, Department of Chemistry, Faculty of Sciences, Al-Baath University, Homs, Syria
Received: Apr. 8, 2017;       Accepted: May 22, 2017;       Published: Jul. 13, 2017
DOI: 10.11648/j.jb.20170102.12      View  1536      Downloads  79
Three Dialdehydes were synthesized by the reaction of Salicylaldehyde and many Aliphatic and Aromatic Halides. The optimal condition (Catalysts, Temperature, Time of Reaction and Effect of Solvents) to get a high selective compounds and high yields have been studied. The reactions were followed by using Thin Layer Chromatography (TLC). The synthesized compounds were purified and characterized by means of High Performance Liquid Chromatography (HPLC) and spectroscopy methods: Infrared Spectra (IR), 1 H-NMR, 13C-NMR.
Salicylaldehyde, Heterogeneous Catalysts, Dialdehyde, Aliphatic and Aromatic Halides
To cite this article
Joumaa Merza, Ali Alasmi, Studying the Optimum Conditions for the Synthesis the Derivatives of Salicylaldehyde with Halides Compounds, Journal of Biomaterials. Vol. 1, No. 2, 2017, pp. 34-39. doi: 10.11648/j.jb.20170102.12
Copyright © 2017 Authors retain the copyright of this article.
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